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有机化合物结构鉴定:光谱数据手册(英文版)

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  • 大小:87.22 MB
  • 语言:英文版
  • 格式: PDF文档
  • 类别:化学书籍
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关键词:光谱   手册   主编   英文   鉴定
资源简介
有机化合物结构鉴定:光谱数据手册(英文版)
出版时间:2012年版
内容简介
《有机化合物结构鉴定:光谱数据手册(英文版)(原著第4版?修订扩展版)》内容简介:第4版新增了20%实验数据,增添了19F和31PNMR两个章节,以及一些重要的Raman光谱。《有机化合物结构鉴定(英文版)(原著第4版?修订扩展版)》以独特的表示方式—通过文字、表格、图表、图形—将核心的参考数据以简洁的编汇形式予以呈现,通过实践指导诠释了包括NMR,IR,UV/Vis和质谱数据以及相对应各自的化合物的结构特征。除了光谱使用的常规溶剂,还包含了标准试剂、MALDI和FABMS基质材料、质谱碎片峰的基本规律以及代表性化合物的UV/Vis光谱。《有机化合物结构鉴定(英文版)(原著第4版?修订扩展版)》不仅适用于学生课程学习和练习,而且高级学习者可借此书扩展阅读。同时具有初级光谱知识的技术人员可以使用此书,专业人士还可以使用书中的参考数据处理日常光谱信息解析。
目录
1 Introduction

1.1 Scope and Organization

1.2 Abbreviations and Symbols

2 Summary Tables

2.1 General Tables

2.1.1 Calculation of the Number of Double Bond Equivalents from the Molecular Formula

2.1.2 Properties of Selected Nuclei

2.2 BC NMR Spectroscopy

2.3 IH NMR Spectroscopy

2.4 IR Spectroscopy

2.5 Mass Spectrometry

2 5.1 Average Masses of Naturally Occurring Elements with Masses and Representative Relative Abundances of lsotopes

2.5.2 Ranges of Naturall sotope Abundances of Selected Elements

2.5.3 Isotope Patterns ofNaturally Occurring Elements

2.5.4 Calculationoflsotope Distributions

2.5.5 Isotopic Abundances of Various Combinations of Chlorine, Bromine,Sulfur,and Silicon

2.5.6 Isotope Pattems of Combinations of Cland Br

2.5.7 Indicators of the Presence of Heteroatoms

2.5.8 Rules for Determining the Relative Molecular Weight (Mr)

2.5.9 Homologous Mass Series aslndications of StructuralType

2.5.10 Mass Correlation Table

2.5.11 References

2.6 UV/Vis Spectroscopy

3 Combination Tables

3.1 Alkanes,Cycloalkanes N

3.2 Alkenes,Cycloalkenes N

33 Alkynes

3.4 Aromatic Hydrocarbons

3.5 Heteroaromatic Compounds

3.6 Halogen Compounds

3.7 Oxygen Compounds

3.7.1 Alcohol; and Phenols

3.7.2 Ethers

3.8 Nitrogen Compounds

3.8.1 Amines

3.8.2 Nitro Compounds

3.9 Thiols and Sulfides

3.10 Carbonyl Compounds

3.10.1 Aldehydes

3.10.2 Ketones

3.10.3 CarboxylicAcids

3.10.4 Esters and Lactones

3.10.5 Amides and Lactams

4 13C NMR Spectroscopy

4.1 Alkanes

4.1.1 Chemical Shifts

4.1.2 Coupling Constants

4.1.3 References

4.2 Alkenes

4.2.1 Chemical Shifts

4.2.2 Coupling Constants

4.2.3 References

4.3 Alkynes

4.3.1 Chemical Shifts

4.3.2 Coupling Constants

4.3.3 References

4.4 Alicyclics

4.4.1 Chemical Shifts

4.4.2 Coupling Constants

4.5 Aromatic Hydrocarbons

4.5.1 Chemical Shifts

4.5.2 Coupling Constants

4.5.3 References

4.6 Heteroaromatic Compounds

4.6.1 Chemical Shifts

4.6.2 Coupling Constants

4.7 Halogen Compounds

4.7.1 Fluoro Compounds

4.7.2 Chloro Compounds

4.7.3 Bromo Compounds

4.7.4 Iodo Compounds

4.7.5 References

4.8 Alcohols,Ethers,and Related Compounds

4.8.1 Alcohols

4.8.2 Ethers

4.9 Nitrogen Compounds

4.9.1 Amines

4.9.2 Nitro and Nitroso Compounds

4.9.3 Nitrosamines and Nitramines

4.9.4 Azo and Azoxy Compounds

4.9.5 Imines and Oximes

4.9.6 Hydrazones and Carbodiimides

4.9.7 Nitriles and lsonitriles

4.9.8 Isocyanates,Thiocyanates,andlso thiocyanates

4.10 SulfurCompounds

4.10.1 Tluols

4.10.2 Sulfides

4.10.3 Disulfides and Sulfonium Salts

4.10.4 Sulfoxides and Sulfones

4.10.5 Sulfonic and Sulfinic Acids and Derivatives

4.10.6 Sulfurous and Sulfuric Acid Derivatives

4.10.7 Sulfur-Containing CarbonylDerivatives

4.11 CarbonyICompounds

4.11.1 Aldehydes

4.11.2 Ketones

4.11.3 CarboxylicAcids

4.11.4 Esters and Lactones

4.11.5 Amides and Lactams

4.11.6 Miscellaneous Carbonyl Derivatives

4.12 Miscellaneous Compounds

4.12.1 Compounds with GroupIV Elements

4.12.2 Phosphorus Compounds

4.12.3 Miscellaneous Organometallic Compounds

……

5 H NMR Spectroscopy

6 Heteronuclear NMR Spectroscopy

7 IR Spectroscopy

8 Mass Spectrometry

9 UV/Vis Spectroscopy

Subject Index
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